This blog documents the experiences of economically disadvantaged high students who are conducting undergraduate scientific research at Duquesne University through the American Chemical Society’s Project SEED.
Thursday, July 3, 2014
Another Update on my MOF research
Today I added MgCl2, IPA, and C5H5N5 to a 50%-50% EtOH and H2O solution, sonicated it, and placed it in an 80 degree oven. The last vials I placed in the oven retained no precipitate, so they were thrown away. Hopefully this batch will work better, or at least produce more than nothing. I also did the same with CrCl2 (adding it to IPA and C5H5N5 to the 50%-50% solution, sonicating it, and putting it in the oven at 80 degrees) and I hope I will have better things to report the next time I update. Oh, wait, I forgot! There was a little tiny bit of precipitate in one of my 20mL vials, it was hardly solid, so I was told to repeat the experiment in a 30mL vial. That was placed in a 100 degree oven for the next three days. And the 30mL vials I put in the oven yesterday (MgCl2 and CrCl2, my starting products, mixed with C5H5N5, IPA, and 1.4 CDHA, in a 50-50 solution of EtOH and H2O and then the same starting products and additions, but in a 1.1.1 solution of DMF, EtOH, and H2O. Two of the 50-50 vials dried out, so they had to be filtered. They are filtering as I am writing this.
I just realized that this is probably confusing, because there is a lot of gaps between information. However, I am not going to write this really long, multi-paragraphed update that no one will read all the way through anyway, so I guess I will have to update more than once every four-five days...
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